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20 mM HEPES, 5 mM D-glucose, 145 mM NaCl, 5.4 mM KCl, 1.8 mM CaCl 2 , 1 mM MgCl 2 , 0.8 mM Na 2 HPO 4 , pH adjusted with NaOH at 37 C to 7.4) and incubated at 37 C with 200 L IB containing 100 M of the -glutamyltranspeptidase inhibitor acivicin [40] in the absence or the presence of the compounds indicated in the figures and tables